发明名称 Method of preparing alpha-and-beta-tricalcium phosphate powders
摘要 The invention describes a wet-chemical process for the preparation of alpha- and beta-tricalcium phosphate (TCP) powders. The procedure simply comprises immediate addition of di-ammonium hydrogen phosphate to an aqueous solution of calcium nitrate tetrahydrate, or vice versa. Calcination of the recovered precursor powders at 800° C. in air produces beta-TCP, whereas the calcination of the same at 1200° C., followed by rapid cooling to room temperature yields submicron-particulated alpha-TCP powders. These powders can be the raw materials for bioceramics, such as artificial bones, artificial joints, artificial tooth roots, and calcium phosphate-based self-setting, self-hardening cements.
申请公布号 US2003235622(A1) 申请公布日期 2003.12.25
申请号 US20030465595 申请日期 2003.06.20
申请人 MERCK PATENT GMBH 发明人 TAS AHMET CUNEYT
分类号 A61L27/00;C01B25/32;(IPC1-7):A61K33/42;C01B15/16;C01B25/26 主分类号 A61L27/00
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