发明名称 METHOD FOR PREPARING 1-PHENYL-1-(ALKYL)PHENYL- ACETONES
摘要 FIELD: organic chemistry, chemical technology. SUBSTANCE: invention relates to method for preparing 1-phenyl-1-(alkyl)phenylacetones of the general formula: RnC6H5-nCH(C6H5)COCH3 wherein R means alkyl; n = 1-3. Method involves preparing firstly the complex 1-chloro-1- phenylacetone with aluminum chloride in methylene chloride or chloroform, or carbon tetrachloride at temperature 30 C, not above, followed by its interaction with alkylbenzene at temperature 30-50 C. Method provides elimination of disproportionation reaction of alkylbenzenes. EFFECT: improved preparing method, enhanced quality and yield of end product. 1 tbl, 1 ex
申请公布号 RU2214389(C2) 申请公布日期 2003.10.20
申请号 RU20010124365 申请日期 2001.09.04
申请人 ZAKRYTOE AKTSIONERNOE OBSHCHESTVO "SHCHELKOVO AGRO;SHCHELKOVO AGRO AOZT 发明人 NAUMOV JU.A.;CHERNYSHEV V.P.;KOVALEVA A.S.;KARAKOTOV S.D.;JURINA V.S.;SHKOLINA L.A.;KOVALENKO O.M.
分类号 C07C45/46;C07C49/215;(IPC1-7):C07C45/46 主分类号 C07C45/46
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