发明名称 METHOD FOR PREPARING SILVER HALIDE EMULSION, SILVER HALIDE EMULSION AND SILVER HALIDE PHOTOGRAPHIC SENSITIVE MATERIAL
摘要 PROBLEM TO BE SOLVED: To provide a silver halide emulsion having an improved grain size distribution, a reduced proportion of non-tabular multiple twin grains and improved sensitivity, graininess, preservability and production lot reproducibility. SOLUTION: In a method for preparing a silver halide emulsion, crystal formation of grains is carried out in a reactive solution containing a dispersion medium, and while the reactive solution during crystal formation is heated, (a) a silver halide solvent is added and aging is carried out, (b) silver ions and halide ions are supplied and grain growth is carried out, (c) the pH is adjusted to 8.0-14.0 and then adjusted to 1.0 to <8.0, (d) average mixing time T<SB>1</SB>in nuclei formation and average mixing time T<SB>2</SB>in the aging and growth satisfy the relation of 0<T<SB>1</SB>/T<SB>2</SB><1, and (e) concentration and addition of water are carried out under heating and cooling during the grain growth. COPYRIGHT: (C)2003,JPO
申请公布号 JP2003255481(A) 申请公布日期 2003.09.10
申请号 JP20020054745 申请日期 2002.02.28
申请人 KONICA CORP 发明人 KONDO AKIYA;ISHIKAWA SADAYASU
分类号 G03C1/015;G03C1/035;(IPC1-7):G03C1/015 主分类号 G03C1/015
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