发明名称 METHOD OF PURIFYING 4-AMINOPIPERIDINES WITH A SPATIAL OBSTACLE
摘要 PCT No. PCT/EP97/02822 Sec. 371 Date Nov. 12, 1998 Sec. 102(e) Date Nov. 12, 1998 PCT Filed May 30, 1997 PCT Pub. No. WO97/46529 PCT Pub. Date Dec. 11, 1997A process for purifying crude piperidines of the formula I where R1 to R4 are C1-C6-alkyl, or R1 and R2 and/or R3 and R4 together are a CH2-chain of 2 to 5 carbons, which comprises, in a first step, removing high-boiling substances and, if present, water from the crude piperidines by distillation; in a second step, adding from 0.01 to 5% by weight, based on the product of the first step, as a reducing agent; and, in a third step, isolating the piperidines by distillation.
申请公布号 PL185707(B1) 申请公布日期 2003.07.31
申请号 PL19970330278 申请日期 1997.05.30
申请人 BASF AG 发明人 JULIUS MANFRED;RUST HARALD;KRAUSE ALFRED;SIEGEL HARDO;SIEGEL WOLFGANG;WITZEL TOM
分类号 C07D211/58;C07D211/56 主分类号 C07D211/58
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