发明名称 METHOD FOR PRODUCING THIOCARBOXYLIC ACID AND ITS SALT, METHOD FOR MEASURING OPTICAL PURITY THEREOF AND TETRAHYDROFURAN THIOCARBOXYLIC ACID AND ITS DERIVATIVE
摘要 PROBLEM TO BE SOLVED: To provide an industrially easily applicable, simpler and more effective method for producing a high-purity thiocarboxylic acid and its salt and causing little environmental influence, and to provide an easily applicable and simple method for measuring optical purity of an optically active tetrahydrofuran thiocarboxylic acid. SOLUTION: The thiocarboxylic acid or its salt is produced by reacting an acid halide or acid anhydride with a metal salt of hydrogen sulfide in the presence of a base. The optical purity of an optically active tetrahydrofuran thiocarboxylic acid is measured by alkyl-esterifying the optically active tetrahydrofuran thiocarboxylic acid and analyzing by chromatography using an optically active column. COPYRIGHT: (C)2003,JPO
申请公布号 JP2003206274(A) 申请公布日期 2003.07.22
申请号 JP20020319535 申请日期 2002.11.01
申请人 TORAY IND INC 发明人 ISHIKAWA MAMORU;NISHIMURA KAZUAKI
分类号 B01J20/291;C07B53/00;C07B61/00;C07C327/06;C07C327/16;C07D307/24;G01N30/06;G01N30/26;G01N30/74;G01N30/86;G01N30/88;(IPC1-7):C07C327/06;G01N30/48 主分类号 B01J20/291
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