发明名称 PROCESS FOR PREPARING 2,4-DIAMINO-6-(2-METHYL-1-IMIDAZOL)-S-TRIAZINE
摘要 PURPOSE: A process for preparing 2,4-diamino-6-(2-methyl-1-imidazol)-S-triazine is provided, thereby the 2,4-diamino-6-(2-methyl-1-imidazol)-S-triazine can be cheaply prepared in higher yield without producing waste organic solvent. CONSTITUTION: The process for preparing 2,4 - diamino - 6 -(2 - methyl - 1 - imidazol) - S - triazine comprises the steps of: reacting 2-methyl imidazol with acrylonitrile to prepare 1-(β-cyano ethyl)-2-methyl imidazol; and reacting 1-(β-cyano ethyl)-2-methyl imidazol which is not separated from the starting compounds with dicyano diamide to prepare 2,4-diamino-6-(2-methyl-1-imidazol)-S-triazine, wherein the second reaction is carried out in the presence of sodium hydroxide; and the amount of sodium hydroxide used is 0.1 to 0.2 moles per 1 mole of 1-(β-cyano ethyl)-2-methyl imidazol.
申请公布号 KR20030021596(A) 申请公布日期 2003.03.15
申请号 KR20010054940 申请日期 2001.09.07
申请人 LEE, HWAN KWANG 发明人 LEE, HWAN KWANG
分类号 C07D403/06;(IPC1-7):C07D403/06 主分类号 C07D403/06
代理机构 代理人
主权项
地址