发明名称 METHOD FOR PREVENTING VINYLSULFONE COMPOUND FROM QUALITY DETERIORATION AND METHOD FOR PURIFYING THE SAME
摘要 PROBLEM TO BE SOLVED: To provide a method for preventing a vinylsulfone compound from quality deterioration even if a large quantity thereof is subjected to filtration treatment, and to provide a method for industrially purifying the vinylsulfone compound. SOLUTION: This method for preventing the vinylsulfone compound from quality deterioration comprises making a filtration treatment of a solution in the presence of a compound of general formula [2] [where, R<1> is a lower alkyl, lower alkoxy or OH; R<2> is H or a lower alkyl; and Z is H, a lower alkyl or group of general formula [3] (where, R<3> is a lower alkyl, lower alkoxy or OH; and R<4> is H or a lower alkyl)]; wherein the solution is prepared by dissolving the crudely crystallized vinylsulfone compound of general formula [1]: H2 C=CHSO2 -A-SO2 CH=CH2 (where, A is a bivalent hydrocarbon group optionally bearing heteroatom) in a water-miscible organic solvent.
申请公布号 JP2003040858(A) 申请公布日期 2003.02.13
申请号 JP20010228428 申请日期 2001.07.27
申请人 WAKO PURE CHEM IND LTD;FUJI PHOTO FILM CO LTD 发明人 TAMURA ATSUSHI;IKEGAWA AKIHIKO
分类号 G03C1/30;C07C315/06;C07C317/44;(IPC1-7):C07C315/06 主分类号 G03C1/30
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