发明名称 |
METHOD FOR MAKING HYDROPHOBIC SILICA GELS UNDER NEUTRAL CONDITIONS |
摘要 |
<p>The present invention is hydrophobic silica gels and a method for their preparation under neutral conditions. The method comprises two steps, where in the first step the pH of a silica hydrosol is adjusted with a base to within a range of about pH 3 to pH 7 to facilitate formation of a silica hydrogel. In the second step the silica hydrogel is contacted with an organosilicon compound in the presence of a catalytic amount of a strong acid to effect hydrophobing of the silica hydrogel. In a preferred method, in a third step the hydrophobic silica gel is contacted with a sufficient quantity of a water-immiscible organic solvent to convert the hydrophobic silica hydrogel into a hydrophobic silica organogel.</p> |
申请公布号 |
EP0963346(B1) |
申请公布日期 |
2003.01.22 |
申请号 |
EP19980910011 |
申请日期 |
1998.02.18 |
申请人 |
DOW CORNING CORPORATION |
发明人 |
BURNS, GARY, T.;DENG, QIN;HAHN, JAMES, R.;REESE, CLIFFORD, C. |
分类号 |
C01B33/159;C08K9/06;C09C1/28;C09C3/12;(IPC1-7):C01B33/16;C09C1/30 |
主分类号 |
C01B33/159 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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