发明名称 METHOD FOR PRODUCING (R,S)-N-BENZYLE-2-(4-FLUORO-3- TRIFLUOROMETHYLPHENOXY)BUTAMAMIDE
摘要 PROBLEM TO BE SOLVED: To provide a method for producing (R,S)-N-benzyl-2-(4-fluoro-3- trifluoromethylphenoxy)butanamide by which operating efficiency is excellent with high yield and a crystallizing solvent to be used is reduced in crystallization of the (R,S)-N-benzyl-2-(4-fluoro-3-trifluoromethylphenoxy) butanamide. SOLUTION: A concentration residue of a reactional liquid for synthesizing the (R,S)-N-benzyl-2-(4-fluoro-3-trifluoromethylphenoxy)butanamide is mixed with an aprotic solvent and a protic solvent in a specific proportion to the aprotic solvent to thereby crystallize the (R,S)-N-benzyl-2-(4-fluoro-3- trifluoromethylphenoxy)butanamide. In the crystallization, the yield is high and operating efficiency is excellent. Furthermore, the crystallizing solvent to be used can be reduced.
申请公布号 JP2003012623(A) 申请公布日期 2003.01.15
申请号 JP20010205639 申请日期 2001.07.06
申请人 UBE IND LTD 发明人 FUKUDA SHOHEI;HOSHIIDE FUMITOSHI
分类号 B01D9/02;C07C231/02;C07C231/24;C07C235/20;(IPC1-7):C07C231/24 主分类号 B01D9/02
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