发明名称 PROCESS FOR OBTAINING AQUEOUS POLYMER DISPERSIONS
摘要 The process comprises the following phases : formation of a pre-emulsion of monomers in water ; transfer into the polymerisation reactor with stirring, of (1) reaction stock consisting of a water solution of a surfactant, in an amount by weight relative to the weight of final polymer dispersion of 1 - 1 5% ; (2) a portion of the pre-emulsion prepared in the previous phase, in an amount of 1% - 10% by weight of the initial pre-emulsion ; phase C.1 : initiation of the polymerisation ; phase C.2 : polymerisation of the monomer mixture at 30 - 90~C, by gradually adding into the reactor, separately, the initiator solution and the remaining portion of the pre-emulsion with an add ed salt, which is soluble in water at 25~C to at least 1% by weight, in an amou nt so as to have a salt concentration in the added pre-emulsion of 0.02 - 0.25% by weight ; phase C.3 : scrubbing of the residual monomers.
申请公布号 CA2447131(A1) 申请公布日期 2002.11.21
申请号 CA20022447131 申请日期 2002.05.17
申请人 ATOFINA 发明人 SAIJA, LEO MARIO;FINOCCHIARO, STEFANO;BECCHI, DANIELE;LUGLI, MARIO
分类号 C08F2/00;C08F2/22;(IPC1-7):C08F2/22 主分类号 C08F2/00
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