发明名称 METHOD FOR PREPARING EPOXIDE CRYSTAL
摘要 PROBLEM TO BE SOLVED: To provide a method for preparing (2R,3S)-3-tert- butoxycarbonylamino-1,2-epoxy-4-phenylbutane((2R,3S)-epoxide form) and (2S,3 R)-3-tert-butoxycarbonylamino-1,2-epoxy-4-phenylbutane((2S,3R)-epoxide form) simply, without requiring very low-temperature condition and in a high recovering ratio. SOLUTION: In to a polar solvent solution dissolving the (2R,3S)-epoxide form or the (2S,3R)-epoxide form, crystallization of the desired epoxide is conducted by adding water.
申请公布号 JP2002322166(A) 申请公布日期 2002.11.08
申请号 JP20010377418 申请日期 2001.12.11
申请人 AJINOMOTO CO INC 发明人 SUZUKI YUICHI;HIROSE NAOKO;ONISHI TOMOYUKI;IZAWA KUNISUKE
分类号 C07D301/32;C07D301/26;C07D303/36;(IPC1-7):C07D301/32 主分类号 C07D301/32
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