发明名称 Method of preparing alkaloids using supercritical fluids from plants
摘要 The invention relates to a method for extracting and preparing alkaloids from plants using supercritical fluid extracting technology and alkaloids prepared by said method. Specifically, the invention relates to a method of preparing alkaloids by mixing plants with carbon dioxide as a major solvent and 1 to 20 parts by weight of at least one alkaline cosolvent selected from a group consisting of methanol, ethanol, water or a mixture thereof wherein 2 to 18 (v/v) % of diethylamine or triethylamine is dissolved in the cosolvent based on 100 parts by weight of carbon dioxide at the temperature of 70 to 90° C. and under 4000 to 6000 PSI of pressure in a supercritical extracting apparatus to extract the alkaloid, and then separating, filtering and purifying the alkaloid using the chromatography, and to alkaloids prepared by said method.
申请公布号 US2002165392(A1) 申请公布日期 2002.11.07
申请号 US20010792306 申请日期 2001.02.23
申请人 KIM JIN WOONG;CHOI YOUNG HAE;YOO KI PUNG;NOH MIN JEONG;HAN JOO HEE 发明人 KIM JIN WOONG;CHOI YOUNG HAE;YOO KI PUNG;NOH MIN JEONG;HAN JOO HEE
分类号 C07D491/22;C07D471/08;C07D491/18;(IPC1-7):C07C211/00 主分类号 C07D491/22
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