发明名称 Preparation of 2-alkyl-3-(4,5-dihydroisoxazol-3-yl) halobenzenes
摘要 A novel process for preparing the compounds of the formula I where: n is 0, 1 or 2; R1,R2 are C1-C6-alkyl; R3,R4,R5 are hydrogen or C1-C6-alkyl, or R4 and R5 together form a bond; R6 is Cl, Br, which comprises a synthesis sequence starting from 1,2-dialkylbenzenes of the formula II with subsequent halogenation to give 3,6-dihalo-1,2-dialkylbenzenes, haloalkylation to give benzyl bromides, oxidation to give benzaldehydes, oximation, reaction 40 with alkenes to give isoxazoles, conversion into thioethers and, if appropriate, oxidation to give sulfenyl or sulfonyl derivatives of the formula I.
申请公布号 US2002156290(A1) 申请公布日期 2002.10.24
申请号 US20020141236 申请日期 2002.05.09
申请人 RACK MICHAEL;GOTZ NORBERT;HAGEN HELMUT;DEYN WOLFGANG VON;BAUMANN ERNST;LOCHTMAN RENE;GEBHARDT JOACHIM 发明人 RACK MICHAEL;GOTZ NORBERT;HAGEN HELMUT;DEYN WOLFGANG VON;BAUMANN ERNST;LOCHTMAN RENE;GEBHARDT JOACHIM
分类号 C07D261/04;(IPC1-7):C07D261/02;C07D261/06 主分类号 C07D261/04
代理机构 代理人
主权项
地址