发明名称 Method of purifying N-(2-hydroxyethy)-2- pyrrolidone
摘要 A method for obtaining high purity N-(2-hydroxyethyl)-2-pyrrolidone satisfactory for use as an intermediate material for N-vinyl-2-pyrrolidone from a reaction liquid formed of a reaction between y-butyrolactone and 2-aminoethanol, i.e., a liquid containing N-(2-hydroxyethyl)-2-pyrrolidone, compounds having boiling points lower than that of N-(2-hydroxyethyl)-2-pyrrolidone and compounds having boiling points higher than that of N-(2-hydroxyethyl)-2-pyrrolidone. The method is characterized by distilling said reaction liquid using a distillation column, whereby obtaining a liquid containing the compounds having the lower boiling points than that of N-(2-hydroxyethyl)-2-pyrrolidone and N-(2-hydroxyethyl)-2-pyrrolidone as a distillate liquid from the column top and a liquid containing compounds having boiling points higher than that of N-(2-hydroxyethyl)-2-pyrrolidone as a bottom liquid.
申请公布号 US2002139657(A1) 申请公布日期 2002.10.03
申请号 US20020105447 申请日期 2002.03.26
申请人 NIPPON SHOKUBAI CO., LTD. 发明人 UGAMURA SHUKICHI;SUGIURA HIDETO;YANO HITOSHI
分类号 C07D207/26;C07D207/27;(IPC1-7):B01D3/10 主分类号 C07D207/26
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