发明名称 PROCEDE DE PREPARATION DE BENZOYLACRYLATES D'ALKYLE
摘要 Process for the preparation of alkyl benzoylacrylates of formula (I) where R = alkyl, in which the reaction is carried out in an acid medium in the same reactor, without isolating the intermediate products, as follows: condensation of acetophenone with glyoxylic acid, elimination of a water/acetophenone mixture, elimination of the excess acetophenone, esterification with an alcohol in the presence of a strong acid, addition of a solvent, elimination of a mixture constituted by water, solvent and alcohol, dehydration by azeotropic distillation of the water, neutralization of the strong acid with a basic aqueous solution, decanting and concentration of the organic phase and recovery of the sought final product of formula (I).
申请公布号 FR2821353(A1) 申请公布日期 2002.08.30
申请号 FR20010002572 申请日期 2001.02.26
申请人 CLARIANT 发明人 SIDOT CHRISTIAN
分类号 C07C67/327;C07C67/08;C07C69/533;(IPC1-7):C07C69/738 主分类号 C07C67/327
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