发明名称 METHOD FOR PRODUCING S,S-ETHYLENEDIAMINE-N,N-DISUCCINIC ACID IRON AMMONIUM CRYSTAL
摘要 PROBLEM TO BE SOLVED: To provide a method for producing an EDDS iron complex crystal, suitable for mass production, having excellent productivity, with which an EDDS iron complex crystal can be continuously produced in a high yield by a simple operation. SOLUTION: This method for an EDDS iron complex crystal comprises a first process for concentrating an aqueous solution S,S-ethylenediamine-N,N- disuccinic acid iron ammonium (EDDS iron complex for short) under reduced pressure and crystallizing a part of the EDDS iron complex to give a slurry, a second process for supplying an aqueous solution of the EDDS iron complex to the slurry while concentrating the slurry under reduced pressure, continuously crystallizing the EDDS iron complex, taking out a part of the slurry and maintaining the volume of the slurry always constant and a third process for separating the taken out slurry into a crystal and a mother liquor and recovering them.
申请公布号 JP2002241354(A) 申请公布日期 2002.08.28
申请号 JP20010038532 申请日期 2001.02.15
申请人 MITSUBISHI RAYON CO LTD 发明人 KANEKO ISAO;BANBA HIROYASU;NIWA KIYONOBU
分类号 C07C227/42;C07C229/76;(IPC1-7):C07C227/42 主分类号 C07C227/42
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