发明名称 |
Process for producing epsi-caprolactam |
摘要 |
A high purity epsi-caprolactam is prepared by pouring a molten crude epsi-caprolactam and a solvent comprising an aliphatic hydrocarbon and having a lower temperature than that of the crude epsi-caprolactam, into a vessel and mixing them to obtain a first slurry containing a crystallized epsi-caprolactam. The slurry is then subjected to a solid-liquid separation to obtain epsi-caprolactam and a first liquid phase. This process can effectively remove impurities from a crude epsi-caprolactam, which is obtained by for example, subjecting cyclohexanone oxime to the Beckmann rearrangement.
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申请公布号 |
US6433166(B2) |
申请公布日期 |
2002.08.13 |
申请号 |
US20010887360 |
申请日期 |
2001.06.25 |
申请人 |
SUMITOMO CHEMICAL COMPANY, LIMITED |
发明人 |
SHIMAZU YASUMOTO;UMIDA HIROYUKI;FUKAO MASAMI |
分类号 |
C07D223/10;C07B61/00;C07D201/16;(IPC1-7):C07D201/16 |
主分类号 |
C07D223/10 |
代理机构 |
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代理人 |
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地址 |
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