发明名称 METHOD OF SYNTHESIS OF N-[(2,3-FULLERENE[60]-2,3-DIHYDRO-1H-1,2,3- BENZOTRIAZOLE-1-YL]-N,N-DIMETHYL-AMINE
摘要 organic chemistry, chemical technology. SUBSTANCE: invention relates to a method of synthesis of functionally substituted fullerene, namely: N-[(2,3-(fullerene[60]-2,3-dihydro-1H-1,2,3-benzotriazole-1-yl]-N,N- dimethylamine of the formula (I) that can be used as a chelating agent, sorbent of biologically active compound. Method involves interaction of fullerene[60] with 5-15-fold excess of N-[(1,2,3-benzotriazole-1-yl)-methyl] -N,N-dimethylamine in argon atmosphere, in toluene medium at 190-210 C for 6-10 h. The yield of the end product is 72-88%. EFFECT: improved method of synthesis, high yield. 1 cl, 1 tbl, 1 ex
申请公布号 RU2183634(C2) 申请公布日期 2002.06.20
申请号 RU20000124496 申请日期 2000.09.25
申请人 INSTITUT NEFTEKHIMII I KATALIZA AN RB I UNTS RAN 发明人 DZHEMILEV U.M.;IBRAGIMOV A.G.;SHARIPOVA F.V.;TUKTAROV R.F.;ABZALIMOV R.R.;SPIRIKHIN L.V.
分类号 C07D487/04;C01B31/02;(IPC1-7):C07D487/04 主分类号 C07D487/04
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