摘要 |
organic chemistry, chemical technology. SUBSTANCE: invention relates to a method of synthesis of functionally substituted fullerene, namely: N-[(2,3-(fullerene[60]-2,3-dihydro-1H-1,2,3-benzotriazole-1-yl]-N,N- dimethylamine of the formula (I) that can be used as a chelating agent, sorbent of biologically active compound. Method involves interaction of fullerene[60] with 5-15-fold excess of N-[(1,2,3-benzotriazole-1-yl)-methyl] -N,N-dimethylamine in argon atmosphere, in toluene medium at 190-210 C for 6-10 h. The yield of the end product is 72-88%. EFFECT: improved method of synthesis, high yield. 1 cl, 1 tbl, 1 ex
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