发明名称 |
NEUTRAL-GEALTERTE, HYDROPHOBISCHE ORGANOSILIKAT-MODIFIZIERTE KIESELSÄUREGELE |
摘要 |
The present invention is neutral-aged hydrophobic organosilicate-modified silica gels and a method for their preparation. The method comprises three steps, where in the first step an organosilicate-modified silica hydrosol is contacted with a strong mineral acid at a pH less than about 1 to form an organosilicate-modified silica hydrogel. In the second step the organosilicate-modified silica hydrogel is aged at a pH within a range of about pH 3.5 to pH 8. In the third step the neutral-aged organosilicate-modified silica hydrogel is contacted with an organosilicon compound in the presence of a catalytic amount of a strong acid to effect hydrophobing of the organosilicate-modified silica hydrogel to form a hydrophobic organosilicate-modified silica hydrogel having a surface area within a range of about 100 m2/g to 750 m2/g in the dry state. In a preferred process the hydrophobic organosilicate-modified silica hydrogel is contacted with a sufficient quantity of a water-immiscible organic solvent to convert the hydrophobic organosilicate-modified silica hydrogel into a hydrophobic organosilicate-modified silica organogel. |
申请公布号 |
DE69804774(D1) |
申请公布日期 |
2002.05.16 |
申请号 |
DE1998604774 |
申请日期 |
1998.02.18 |
申请人 |
DOW CORNING CORP., AUBURN |
发明人 |
BURNS, T.;DENG, QIN;HAHN, R.;REESE, C. |
分类号 |
C01B33/159;C01B33/16;C09C1/30;(IPC1-7):C01B33/16 |
主分类号 |
C01B33/159 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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