发明名称 METHOD OF MANUFACTURING THERMOSTABLE CARBON
摘要 PROBLEM TO BE SOLVED: To provide a method of mass-producing a thermostable carbon whose process is simple and carried out at low temperature in atmospheric pressure using a conventional apparatus. SOLUTION: The thermostable carbon is manufactured by the following processes: The catalyst 3 which is prepared by a sol-gel method and comprises 30 wt.% Ni-SiO2 is filled into the reaction tube 1, heated at 500 deg.C by the electric furnace 7 and preliminarily reduced for 1 hr by gaseous hydrogen whose flow rate is 50 ml/min. Then the gas mixture of hydrogen and carbon dioxide whose mixing ratio is 2 to 1 is passed through in the reaction tube 1 with space velocity of 7000/hr for 30 min. Carbon dioxide in the gas mixture is catalytically- reduced with hydrogen by coming in contact with the catalyst 3 to deposit the thermostable carbon on the catalyst surface.
申请公布号 JP2002104815(A) 申请公布日期 2002.04.10
申请号 JP20000298818 申请日期 2000.09.29
申请人 SHIMADZU CORP 发明人 ONO SHIGEKI
分类号 C01B31/02;B01J23/755;B01J23/89;C09K3/16;C09K3/18 主分类号 C01B31/02
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