发明名称 |
METHOD FOR PREPARING ALUMINUM NITRIDE POWDER BY SELF-PROPAGATING HIGH TEMPERATURE SYNTHESIS |
摘要 |
PURPOSE: A method for preparing aluminum nitride powder with high purity and chemical stability by self-propagating high temperature synthesis is provided. CONSTITUTION: The preparation method of aluminum nitride powder includes the steps of (i) mixing 30-80wt.% of metal aluminum powder with a particle size of less than 100μm with 20-70wt.% of aluminum nitride until its density reaches 20-50% of theoretical density; (ii) keeping the reaction system under a nitrogen atmosphere ranging from 1 to 50 atm; (iii) by applying high voltage to a hot wire, elevate the temperature of a mixture of metal aluminum powder and aluminum nitride powder to a temperature where self-propagating high temperature synthesis start; and (iv) crushing obtained aluminum nitride lump. In the first step, 1-40wt.% of a mixture containing carbon powder, halogen compounds of 1 group, 2 group, and 3 group or their hydrate is further added, based on the total weight of the mixture.
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申请公布号 |
KR20020023570(A) |
申请公布日期 |
2002.03.29 |
申请号 |
KR20000055941 |
申请日期 |
2000.09.23 |
申请人 |
KAM TECHNOLOGY CORPORATION |
发明人 |
CHO, JONG MUK;JUNG, IN BEOM;KIM, RAE EUN;KIM, YONG SEOK;LIM, DONG SU |
分类号 |
C01B21/06;(IPC1-7):C01B21/06 |
主分类号 |
C01B21/06 |
代理机构 |
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