发明名称 |
METHOD FOR THE PRODUCTION OF DOLLAR G(V)-AMINOALKYLSULPHONIC ACIDS |
摘要 |
The invention relates to a method for the production of OMEGA -aminoalkylsulphonic acids of general formula (I), where R1 and R2 = optionally substituted alkyl groups with 1 20 C atoms and n = a whole number from 2 6, whereby an amine of formula (II), where R1 and R2 have the above meanings is reacted with an alkyl dihalide of formula (III), where n has the above meaning and X1 and X2 = chlorine or bromine, with addition of alkali hydroxide at a pH of 8 10. The pH is then adjusted to a value of 0 1, by addition of a hydrohalic acid and excess alkyl dihalide is separated off, before the reaction solution is adjusted to a pH of 6 7.5 with alkali liquor, alkali sulphite is added and the product (I) formed at elevated temperate. |
申请公布号 |
WO0185678(A1) |
申请公布日期 |
2001.11.15 |
申请号 |
WO2001EP04754 |
申请日期 |
2001.04.27 |
申请人 |
RASCHIG GMBH;SCHAEFER, VOLKER;KNOLL, WOLFGANG;SCHMITT, ALEXANDER;HUETTNER, CHRISTOPH |
发明人 |
SCHAEFER, VOLKER;KNOLL, WOLFGANG;SCHMITT, ALEXANDER;HUETTNER, CHRISTOPH |
分类号 |
C07C303/02;C07C303/44;C07C309/14;C07D295/088 |
主分类号 |
C07C303/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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