发明名称 Process for purifying L-ascorbyl 2-monophosphate
摘要 A process for separating L-ascorbyl 2-monophosphate from a mixture of the products of the desalting of the product mixture obtained from the phosphorylation under basic conditions of an L-ascorbic acid salt is described. This process is characterized by passing an aqueous solution of the desalted mixture containing among other components the desired L-ascorbyl 2-monophosphate through a column of a basic anion exchange resin, with resulting adsorption of the components onto the resin, desorbing among other adsorbed components the L-ascorbyl 2-monophosphate from the resin using as the eluent an aqueous alkali hydroxide solution, and collecting from the eluate the fraction which contains as its principal dissolved component the desired L-ascorbyl 2-monophosphate in the form of the appropriate mono-alkali metal salt. The so obtained L-ascorbyl 2-monophosphate is especially stable against thermal and oxidative degradation compared with L-ascorbic acid (vitamin C) itself, and is thus suitable as a more stable form of ascorbic acid for use as an additive for foodstuffs, animal feeds and cosmetic products.
申请公布号 US6288243(B1) 申请公布日期 2001.09.11
申请号 US20000583254 申请日期 2000.05.31
申请人 ROCHE VITAMINS INC. 发明人 NOESBERGER PAUL
分类号 B01D15/00;B01D15/04;B01J41/04;C07F9/09;C07F9/655;(IPC1-7):C07F9/06 主分类号 B01D15/00
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