发明名称 METHOD OF MANUFACTURING FOR LONG CHAIN ALIPHATIC AMINE OXIDE
摘要 PROBLEM TO BE SOLVED: To provide a method of manufacturing for a long chain aliphatic amine oxide having a good color tone and low in residual hydrogen peroxide using only water without using an aqueous solvent such as an alcohol or the like. SOLUTION: In this method manufacturing a long chain aliphatic amine oxide by reacting a tertiary amine expressed by general formula (I) (R1 is an alkyl group or alkenyl group having 16-24 carbon atoms of straight or branched chain, R2 and R3 are each an alkyl group or hydroxyethyl group having same or different 1-3 carbon atoms.) and hydrogen peroxide to manufacture the corresponding amine oxide, only water is used as a solvent, in the oxidizing reaction, and the agitating speed is reduced to set the agitating power at 0.03-0.30 kW/m3 when the reaction rate reaches to 50-90%, and then continuing the reaction by increasing the agitating force again after dissolving gel in the reaction liquid.
申请公布号 JP2001213859(A) 申请公布日期 2001.08.07
申请号 JP20000023825 申请日期 2000.02.01
申请人 LION AKZO KK 发明人 SATO AKIHIRO;WAKUI TSUGIO
分类号 C11D1/75;C07C291/04;(IPC1-7):C07C291/04 主分类号 C11D1/75
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