发明名称 |
METHOD FOR PRODUCING ACRYLIC SYRUP |
摘要 |
PROBLEM TO BE SOLVED: To provide a method for producing an acrylic syrup not requiring an inert gas during reaction. SOLUTION: (1) A monomer in an amount of 20-70 wt.% based on the whole amount of a raw material comprising methyl methacrylate as a main component is heated to the boiling point of a composition in a system within 2 hours, (2) a chain transfer agent is added at a point of time when the composition in the system reaches its boiling point and a reflux starts, (3) the monomer in an amount of 80-30 wt.% based on the whole amount of the raw material is continuously or dividedly added for a time selected from a range of 0.1-10 hours while a reaction temperature is set at the boiling point of the composition in the system and the reflux is maintained and (4) a polymerization initiator is continuously or dividedly added simultaneously with the addition of the monomer and the reaction is carried out.
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申请公布号 |
JP2001151801(A) |
申请公布日期 |
2001.06.05 |
申请号 |
JP19990339700 |
申请日期 |
1999.11.30 |
申请人 |
MITSUBISHI GAS CHEM CO INC |
发明人 |
HINAGATA SHINICHI;KAWABATA TADASHI;KUWABARA SHOJIRO;KUROKAWA MASAHIRO |
分类号 |
C08F2/00;C08F20/14;(IPC1-7):C08F2/00 |
主分类号 |
C08F2/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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