发明名称 METHOD FOR PRODUCING ACRYLIC SYRUP
摘要 PROBLEM TO BE SOLVED: To provide a method for producing an acrylic syrup not requiring an inert gas during reaction. SOLUTION: (1) A monomer in an amount of 20-70 wt.% based on the whole amount of a raw material comprising methyl methacrylate as a main component is heated to the boiling point of a composition in a system within 2 hours, (2) a chain transfer agent is added at a point of time when the composition in the system reaches its boiling point and a reflux starts, (3) the monomer in an amount of 80-30 wt.% based on the whole amount of the raw material is continuously or dividedly added for a time selected from a range of 0.1-10 hours while a reaction temperature is set at the boiling point of the composition in the system and the reflux is maintained and (4) a polymerization initiator is continuously or dividedly added simultaneously with the addition of the monomer and the reaction is carried out.
申请公布号 JP2001151801(A) 申请公布日期 2001.06.05
申请号 JP19990339700 申请日期 1999.11.30
申请人 MITSUBISHI GAS CHEM CO INC 发明人 HINAGATA SHINICHI;KAWABATA TADASHI;KUWABARA SHOJIRO;KUROKAWA MASAHIRO
分类号 C08F2/00;C08F20/14;(IPC1-7):C08F2/00 主分类号 C08F2/00
代理机构 代理人
主权项
地址