| 摘要 |
A preparation process of N,N'-dialkylalkanediamine by reacting dihaloalkane with lower alkylamine characterized by carrying out the reaction with controlling the residual amount in the reaction system of haloalkaneamine intermediate represented by the formula (4):wherein R is a lower alkyl group, R1 and R2 are a hydrogen atom or a lower alkyl group, X is a chlorine, bromine or iodine atom, and n is an integer of 2 to 6, and the invention inhibits formation of by-products cyclic dialkyldiamine and trialkylalkanetriamine and can provide desired N,N'-dialkylalkanediamine with a high yield.
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