发明名称 4-HYDROXY-3-ALKOXYBENZALDEHYDE 2, 3-BUTANEDIOL ACETAL COMPOUNDS AND PERFUME COMPOSITION CONTAINING THE COMPOUND AS ACTIVE INGREDIENT
摘要 PROBLEM TO BE SOLVED: To obtain the subject new compound which has remarkably mild and mellow vanilla-like fragrance and flavor in comparison with known vanilla and so on of conventional perfume substances and is useful as an excellent and unique persistent agent for imparting or changing fragrance and flavor in the wide fields of luxury goods, drinks, foods, healthy materials, medicines, and so on. SOLUTION: A compound of formula I (R is a 1 to 4C alkyl), for example, 4-[4R*,5S*-(4,5-dimethyl-L3-dioxoran-2-yl)]-2-methoxyphenol. The compound of formula I is obtained, for example, by reacting (A) a compound of formula II (for example, vanillin) with (B) 2,3-butanediol of meso-isomer, dl-isomer or their mixture in an amount of about 1 to 2 mole times that of the component A in the presence of a catalyst of p-toluenesulfonic acid preferably at 50 to 150 deg.C for about 1 to 10 hr.
申请公布号 JP2001002673(A) 申请公布日期 2001.01.09
申请号 JP19990170917 申请日期 1999.06.17
申请人 T HASEGAWA CO LTD 发明人 HONDA TSUTOMU;OGURO DAICHI;OSADA HIROSHI
分类号 C07D317/22;A61K8/49;A61Q13/00;C11B9/00;(IPC1-7):C07D317/22;A61K7/46 主分类号 C07D317/22
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