发明名称 |
Processing for producing allyl 2-hydroxyisobutyrate |
摘要 |
There is disclosed a process for producing allyl 2-hydroxyisobutyrate useful as a raw material for agrochemicals and pharmaceuticals, which comprises reacting methyl 2-hydroxyisobutyrate with allyl alcohol preferably by means of reactional distillation in the presence of a transesterification catalyst preferably comprising titanium tetramethoxide or titanium tetraisopropoxide under solventless mild reaction conditions including a reaction temperature in the range of 80 to 150 DEG C. and a reaction time in the range of 10 minutes to 12 hours. The process enables efficient and easy production of the objective allyl 2-hydroxxyisobutyrate in high yield and high efficiency without the need of troublesome operations.
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申请公布号 |
US6162946(A) |
申请公布日期 |
2000.12.19 |
申请号 |
US19990387050 |
申请日期 |
1999.08.31 |
申请人 |
MITSUBISHI GAS CHEMICAL COMPANY, INC. |
发明人 |
SHIMA, YOSHIKAZU;ABE, TAKAFUMI |
分类号 |
B01J31/12;C07B61/00;C07C67/03;C07C69/675;(IPC1-7):C07C69/66 |
主分类号 |
B01J31/12 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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