发明名称 STANDARD MATERIAL OF 1-PHENYL-4-(2-PHENYLETHYL)TETRALIN FOR ANALYZING STYRENE OLIGOMER
摘要 PROBLEM TO BE SOLVED: To obtain a new compound useful as an analytical standard material used for qualitative and quantitative analyses of styrene oligomers contained in a polystyrene. SOLUTION: This standard material is a compound of formula I. The compound of the formula I is obtained by usually reducing a compound of formula II obtained by using 3,3-diphenylpropanol as a starting material and passing through various reactions, by a catalytic hydrogenation reaction in a solvent such as hexane, in the presence of a catalyst such as Pd/C, etc., at preferably a room temperature for 1-10 hr to obtain 1-phenyl-4-(2-phenylethyl)tetralin, and separating the stereo isomer of it by a high speed liquid chromatography, etc.
申请公布号 JP2000327597(A) 申请公布日期 2000.11.28
申请号 JP19990313773 申请日期 1999.11.04
申请人 NISSIN FOOD PROD CO LTD 发明人 HIRANO SATORU;KOBAYASHI KAZUHIRO;SAKURAI KEITEN;YAMADA TOSHIHIRO
分类号 G01N31/00;C07B57/00;C07C5/05;C07C7/12;C07C13/48;(IPC1-7):C07C13/48 主分类号 G01N31/00
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