Process for the distillation of crude ester in the DMT/PTA process

摘要

A process for purifying a crude ester containing dimethyl terephthalate, includes flash distilling a mixture including para-xylene and methyl para-toluate, and separating the crude ester into fractions. By separating the crude ester with a distillation column containing structured packing and using a lower bottom temperature, product yield is increased, and the process is made more economical.