发明名称 PRODUCTION OF 4-HYDROXY-2,2,6,6-TETRAMETHYLPIPERIDIN-1-ONE
摘要 PROBLEM TO BE SOLVED: To provide a method for producing 4-hydroxy-2,2,6,6- tetramethylpiperidin-1-one., capable of easily producing the highly pure 4- hydroxy-2,2,6,6-tetramethylpiperidin-1-one by performing only a solid-liquid separation operation without using an oxidation catalyst and without a special purification process such as an extraction process or a recrystallization process after the finish of the reaction. SOLUTION: This method for producing 4-hydroxy-2,2,6,6- tetramethylpiperidin-1-one comprises oxidizing 4-hydroxy-2,2,6,6- tetramethylpiperidine with hydrogen peroxide. Therein, the characteristics comprises using a reaction vessel comprising a synthetic resin or glass for a liquid-contacting portion, and performing the oxidation reaction in the absence of an oxidizing catalyst, adding at least one metal oxide of nickel oxide and manganese oxide to the oxidation reaction product to decompose the residual hydrogen peroxide after the oxidation reaction is finished, and then removing the metal oxide by a solid-liquid separation operation.
申请公布号 JP2000169447(A) 申请公布日期 2000.06.20
申请号 JP19980345116 申请日期 1998.12.04
申请人 HAKUTO CO LTD 发明人 ONISHI NORIHIKO;O SHIGEKI
分类号 C07D211/94;(IPC1-7):C07D211/94 主分类号 C07D211/94
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