发明名称 |
Process for the preparation of a solid precursor material useful for tungsten oxide based electrochromic coatings |
摘要 |
<p>A process for the preparation of a highly stable solid precursor material useful for tungsten oxide based electrochromic coatings comprises: <SL> <LI>a) preparing an aqueous solution of sodium tungstate in deionized water; <LI>b) passing the aqueous solution prepared in step a) through a vertical column containing acidic ion exchange resin to give an elute; <LI>c) collecting the elute from step b) directly into a peroxide as colloidal polytungstate sol with a pH not exceeding 2; <LI>d) stirring the mixture obtained in c) for a period ranging between 30 to 120 minutes to form a peroxypolytungstate solution; <LI>e) mixing an organic acid to said peroxypolytungstate solution as obtained in step d) under reflux conditions at a temperature of 55{C for a time period in the range of 1-2 hours to form a peroxypolytungstate acid derivative; <LI>f) converting said peroxypolytungstate acid derivative to a highly stable solid precursor material by fast vacuum drying; </SL></p> |
申请公布号 |
GB0007256(D0) |
申请公布日期 |
2000.05.17 |
申请号 |
GB20000007256 |
申请日期 |
2000.03.23 |
申请人 |
COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH |
发明人 |
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分类号 |
C07F11/00;G02F1/15 |
主分类号 |
C07F11/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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