发明名称 PRODUCTION OF METAL-FREE PHTHALOCYANINE
摘要 PROBLEM TO BE SOLVED: To industrially, readily and economically produce the subject compound useful as a pigment, etc., in good purity without any by-product such as PCB by reacting o-phthalodinitrile under specific conditions. SOLUTION: (D) o-Phthalodinitrile which is unsubstituted or has a substituent group is reacted in the presence of (B) an inorganic base (e.g. lithium hydroxide) and (C) a ferrocene compound in (A) an alcoholic solvent (e.g. ethylene glycol). Furthermore, the ferrocene compound represented by the formula (R1 and R2 are each a halogen, nitro, formyl or the like) is used as the component C, which is preferably used in an amount within the range of (1/20) to (1/4) based on 1 mol of the component D. The component B is preferably used in an amount within the range of (1/20) to (1/2) based on 1 mol of the component D and the reactional temperature is preferably about 80-180 deg.C.
申请公布号 JP2000129153(A) 申请公布日期 2000.05.09
申请号 JP19980303446 申请日期 1998.10.26
申请人 TOYO INK MFG CO LTD 发明人 SAKAMOTO MARE
分类号 C09B47/067;C09B47/30;(IPC1-7):C09B47/30 主分类号 C09B47/067
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