发明名称 |
Production of para-xylene from an effluent from paraselective toluene disproportionation using a crystallization process combined with simulated moving bed adsorption |
摘要 |
Para-xylene is produced from a paraselective toluene disproportionation reactor, effluent (3) is distilled to eliminate toluene and benzene in at least 2 distillation columns (C1), (C2), and the xylenes (8) are crystallized at least once (10) at between +10 DEG C. and -30 DEG C. The separated mother liquor (14) is adsorbed on a zeolitic sieve in the presence of toluene in a simulated moving bed (15). This latter produces a raffinate (16) containing toluene which is depleted in para-xylene which is distilled in a distillation column (C4), and an extract which is enriched in para-xylene and contains toluene, which is recycled to columns (C1, C2). The para-xylene crystals are purified by washing with toluene and distillation or by partial melting (30) followed by washing with molten high purity para-xylene.
|
申请公布号 |
US6060634(A) |
申请公布日期 |
2000.05.09 |
申请号 |
US19980132771 |
申请日期 |
1998.08.12 |
申请人 |
INSTITUT FRANCAIS DU PETROLE |
发明人 |
MIKITENKO, PAUL;HOTIER, GERARD |
分类号 |
C07C7/00;C07C7/14;C07C15/08;(IPC1-7):C07C7/00;C07C7/12;C07C5/22 |
主分类号 |
C07C7/00 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|