发明名称 Process for the production of 2,5-dimethyl-2,5-di-t-butylperoxy-hexane
摘要 PCT No. PCT/EP97/01937 Sec. 371 Date Oct. 13, 1998 Sec. 102(e) Date Oct. 13, 1998 PCT Filed Apr. 17, 1997 PCT Pub. No. WO97/38974 PCT Pub. Date Oct. 23, 19972,5-dimethyl-2,5-di-t-butylperoxy-hexane is produced by reacting 2,5-dimethyl-1,5-hexadiene with t-butylhydroperoxide under acid catalysis in the presence of an electron pair acceptor Lewis acid in a substantially anhydrous solvent. If one uses technical water-containing t-butylhydroperoxide, the water can be separated, after mixing with the 2,5-dimethyl-1,5-hexadiene, by adding sulfuric acid or calcium chloride and subsequently the electron pair acceptor Lewis acid is added.
申请公布号 US6034280(A) 申请公布日期 2000.03.07
申请号 US19980171233 申请日期 1998.10.12
申请人 PEROXID-CHEMIE GMBH 发明人 HAEGEL, EBERHARD
分类号 B01J31/22;C07B61/00;C07C409/16;(IPC1-7):C07C409/04 主分类号 B01J31/22
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