摘要 |
PCT No. PCT/EP97/01937 Sec. 371 Date Oct. 13, 1998 Sec. 102(e) Date Oct. 13, 1998 PCT Filed Apr. 17, 1997 PCT Pub. No. WO97/38974 PCT Pub. Date Oct. 23, 19972,5-dimethyl-2,5-di-t-butylperoxy-hexane is produced by reacting 2,5-dimethyl-1,5-hexadiene with t-butylhydroperoxide under acid catalysis in the presence of an electron pair acceptor Lewis acid in a substantially anhydrous solvent. If one uses technical water-containing t-butylhydroperoxide, the water can be separated, after mixing with the 2,5-dimethyl-1,5-hexadiene, by adding sulfuric acid or calcium chloride and subsequently the electron pair acceptor Lewis acid is added.
|