发明名称 Isolation and purification of sterols from neutrals fraction of tall oil pitch by direct crystallization, single phase
摘要 Isolation of the sterol component of the neutrals fraction of saponified tall oil pitch is disclosed. To the extracted neutrals, in a hydrocarbon (preferably heptane) phase, are added small amounts of water and an alcohol solvent, preferably methanol, at a relatively high temperature (preferably greater than 70 DEG C). The hydrocarbon/neutrals/alcohol/water solution is allowed to cool slowly, with agitation, to facilitate crystallization of sterols. The sterols are isolated and washed with hydrocarbon solvent.
申请公布号 AU4958699(A) 申请公布日期 2000.03.06
申请号 AU19990049586 申请日期 1999.07.12
申请人 WESTVACO CORPORATION 发明人 PHILIP L. ROBINSON;THOMAS J. CUFF
分类号 C07J9/00;C11B13/00 主分类号 C07J9/00
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