发明名称 PROCESS FOR PRODUCING TRIS (PENTAFLUOROPHENYL) BORANE
摘要 A process for producing tris(pentafluorophenyl)borane which comprises reacting chloropentafluorobenzene with an organometallic compound (formula 1: RM) such as sec-butyllithium in an ether solvent or an ether/hydrocarbon mixed solvent to obtain a pentafluorophenylmetal (formula 2: C6H5M) such as pentafluorophenyllithium and reacting the reaction product with a boron compound (formula 3: BX3) such as boron trichloride. Thus, the target compound is synthesized from inexpensive materials through a small number of steps in a high yield. In the formulae, R represents a C1-10 hydrocarbon group; M represents an alkali metal; and X's may be the same or different and each represents halogeno or alkoxy.
申请公布号 WO9964427(A1) 申请公布日期 1999.12.16
申请号 WO1999JP02974 申请日期 1999.06.03
申请人 ASAHI GLASS COMPANY, LTD.;ASAI, TOMOYUKI;NAKAJIMA, YOSHIKO 发明人 ASAI, TOMOYUKI;NAKAJIMA, YOSHIKO
分类号 C07F5/02;(IPC1-7):C07F1/00;C07F1/02;C07F1/04;C07F1/06 主分类号 C07F5/02
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