发明名称 |
PROCESS FOR PRODUCING TRIS (PENTAFLUOROPHENYL) BORANE |
摘要 |
A process for producing tris(pentafluorophenyl)borane which comprises reacting chloropentafluorobenzene with an organometallic compound (formula 1: RM) such as sec-butyllithium in an ether solvent or an ether/hydrocarbon mixed solvent to obtain a pentafluorophenylmetal (formula 2: C6H5M) such as pentafluorophenyllithium and reacting the reaction product with a boron compound (formula 3: BX3) such as boron trichloride. Thus, the target compound is synthesized from inexpensive materials through a small number of steps in a high yield. In the formulae, R represents a C1-10 hydrocarbon group; M represents an alkali metal; and X's may be the same or different and each represents halogeno or alkoxy.
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申请公布号 |
WO9964427(A1) |
申请公布日期 |
1999.12.16 |
申请号 |
WO1999JP02974 |
申请日期 |
1999.06.03 |
申请人 |
ASAHI GLASS COMPANY, LTD.;ASAI, TOMOYUKI;NAKAJIMA, YOSHIKO |
发明人 |
ASAI, TOMOYUKI;NAKAJIMA, YOSHIKO |
分类号 |
C07F5/02;(IPC1-7):C07F1/00;C07F1/02;C07F1/04;C07F1/06 |
主分类号 |
C07F5/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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