摘要 |
The invention concerns a synthesis method for powder ceramic complexes of refractory metals, which consists in mixing at least an oxide of one of said metals with a reducing metal and with a pure or combined metalloid in solid form, and in heating the resulting mixture to a threshold starting a self-propagating reaction starting temperature so as to obtain said powder ceramics; selecting the particle size of at least one metal oxide on the basis of the desired ceramic particle size; adding, in a specific proportion, at least one of said pure or calcium-combined metalloid, itself added on its own or combined in a specific proportion as metal reducer, and controlling said reaction temperature so as to maintain it at predetermined value, according to the desired particle size distribution for the resulting ceramic complex. |