发明名称 Process for the production of intermediate for liquid crystal compound
摘要 A process for the production of an intermediate for a liquid crystal compound, which comprises reacting an alkyloxybiphenylcarboxylic acid with purified thionyl chloride substantially free of sulfuryl chloride, the thionyl chloride being obtained by adding phenol, etc., to thionyl chloride, heating the mixture and distilling the resultant mixture; and a process for the production of a liquid crystal compound from the above intermediate. According to the present invention, thionyl chloride can be easily purified, and a liquid crystal compound having a very high purity can be obtained by the use of the purified thionyl chloride.
申请公布号 US5939586(A) 申请公布日期 1999.08.17
申请号 US19970962005 申请日期 1997.10.31
申请人 MITSUBISHI GAS CHEMICAL COMPANY, INC. 发明人 MINETA, HIROSHI;YUI, TOMOYUKI
分类号 C01B17/45;C07C51/60;C07C65/24;C07C67/14;C07C69/94;C09K19/20;(IPC1-7):C07C51/58;C07C69/76 主分类号 C01B17/45
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