发明名称 Process for the purification of 5H-dibenz (B,F) azepine
摘要 Process for the purification of 5H-dibenz[b,f]a-zepine, which comprises evaporating 5H-dibenz[b, f]azepine under reduced pressure from a reaction mixture obtained by catalytic dehydrogenation of 10,11-dihydro-5H-dibenz-[b,f]azepine in the 1st step and depositing it as a solid, suspending the deposited product in an aromatic hydrocarbon in the 2nd step and then isolating pure 5H-dibenz[b,f]azepine.
申请公布号 US5895815(A) 申请公布日期 1999.04.20
申请号 US19970942489 申请日期 1997.10.02
申请人 DSM CHEMIE LINZ GMBH 发明人 EICHBERGER, GUENTER;RAML, WALTER
分类号 C07D223/22;C07D223/26;(IPC1-7):C07D223/22 主分类号 C07D223/22
代理机构 代理人
主权项
地址