发明名称 |
Method for continuously producing a cyclic formal |
摘要 |
Cyclic formal is manufactured by cyclic reaction of an alkylene glycol and an aldehyde in a reactor, producing formal mixed with unreacted aldehyde as an impurity, which impurity is reduced in amount by connecting the reactor to a distillation tower and continuously supplying alkylene glycol to the distillation tower from which unreacted formaldehyde and a cyclic formal are being distilled, and continuously reacting them with supplied raw formaldehyde by countercurrent flow during distillation; water content in azeotropic admixture with cyclic formal can be removed by azeotropic distillation with a hydrocarbon azeotropic mixture with water, distilling water from the cyclic formal.
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申请公布号 |
US5886198(A) |
申请公布日期 |
1999.03.23 |
申请号 |
US19980013840 |
申请日期 |
1998.01.27 |
申请人 |
TORAY INDUSTRIES, INC. |
发明人 |
OGAWA, DAISUKE;KOIKE, MASAHIRO;YAMAMOTO, YOSHIYUKI |
分类号 |
C07D317/12;(IPC1-7):C07D307/04 |
主分类号 |
C07D317/12 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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