发明名称 |
PROCESS FOR THE PREPARATION OF 1-ALKOXY-1-TRIMETHYLSILYLOXYCYCLOPROPANES |
摘要 |
<p>The present invention provides a process for producing 1-alkoxy-1-trimethylsilyloxycyclopropane represented by the following general formula: <CHEM> by reacting microgranular metallic sodium dispersed in a hydrocarbon solvent, beta -halogenocarboxylic acid ester represented by the following general formula: <CHEM> and chlorotrimethylsilane. According to the present invention, by using no ether compound solvent (the ether compound solvent has various problems in safety) and using microgranular metallic sodium dispersed in a hydrocarbon solvent, 1-alkoxy-1-trimethylsilyloxycyclopropane can be industrially produced simply (no special apparatus is required) at an advantageous cost at a yield at least equal to that obtained when an ether is used as solvent.</p> |
申请公布号 |
EP0900803(A1) |
申请公布日期 |
1999.03.10 |
申请号 |
EP19970949164 |
申请日期 |
1997.12.19 |
申请人 |
IHARA CHEMICAL INDUSTRY CO., LTD. |
发明人 |
YOSHIDA, YASUO |
分类号 |
C07F7/18;A01N55/00;(IPC1-7):C07F7/18 |
主分类号 |
C07F7/18 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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