摘要 |
Air is separated into oxygen and nitrogen in a double rectification column comprising a higher pressure rectification column and a lower pressure rectification column. Liquid nitrogen reflux for the separation is provided by condensing nitrogen vapor taken from the column in a condenser-reboiler. Additional separation is performed in an intermediate pressure rectification column. A first stream of argon-enriched vapor is withdrawn from an intermediate region of the lower pressure rectification column and has an argon fraction separated from it in a first side rectification column. A second stream of argon-enriched vapor is similarly withdrawn and is separated in a second side rectification column which provides vapor to heat a reboiler associated with the intermediate pressure rectification column. Alternatively a stream of oxygen vapor can be so employed instead of the second argon-enriched vapor stream.
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