发明名称 METHOD OF PREPARING BENZYL CHLORIDE
摘要 FIELD: preparation of medicinal and flavoring agents, and means for protection of plants. SUBSTANCE: benzyl chloride is prepared by hydrochlorination of dibenzyl ether with hydrochloric acid at 90-97 C in the presence of catalyst. Said catalyst is zinc chloride at dibenzyl ether to zinc chloride molar ratio of 1: 1-0.75. Process is carried out when gaseous hydrogen chloride is passed through reaction mixture. Use of readily available and cheap catalyst makes it possible to cut down duration of reaction and to increase by 5-7% yield of the final product. EFFECT: more efficient preparation method. 2 cl, 5 ex, 1 tbl
申请公布号 RU2125035(C1) 申请公布日期 1999.01.20
申请号 RU19970104986 申请日期 1997.04.01
申请人 VOLGOGRADSKOE OTKRYTOE AKTSIONERNOE OBSHCHESTVO "K;HIMPROM 发明人 MUDRYJ F.V.;SPITSYN A.A.
分类号 C07C17/07;C07C22/04;(IPC1-7):C07C17/07 主分类号 C07C17/07
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