发明名称 Process for preparing cellulose ethers with recovery of alkali
摘要 Cellulose ethers which contain hydroxyalkyl groups are prepared, with the recovery of sodium hydroxide, by cellulose being etherified with alkylene oxide in a water-containing organic suspension medium in the presence of at least 1.0 mol of sodium hydroxide per mole of anhydroglucose units, the water-containing organic suspension medium being separated off after the etherification reaction is complete, the crude cellulose ether being extracted with a suitable solvent mixture, the lower-boiling organic components being distilled off from the solvent mixture after the extraction, the water-containing organic suspension medium separated off being added to the distillation residue of the solvent mixture to form a multiphase mixture, the bottom phase of the multiphase mixture being separated and the sodium hydroxide present in the bottom phase being reused.
申请公布号 US5840882(A) 申请公布日期 1998.11.24
申请号 US19970911946 申请日期 1997.08.20
申请人 CLARIANT GMBH 发明人 DOENGES, REINHARD;EHRLER, RUDOLF
分类号 C08B11/02;C08B11/08;C08B11/20;(IPC1-7):C07H1/00;C07H15/08 主分类号 C08B11/02
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