发明名称 Verfahren zur Herstellung von Aminomethanphosphonsäure
摘要 Disclosed is a method for producing amino methane phosphonic acid, whereby a) N monomethylurea is reacted with a phosphorous (III) chloride based phosphorylating reagent at temperatures ranging from 0-90 DEG C in the presence of an organic solvent and b) hydrolyzing the reaction mixture obtained in step a) optionally after removal of the organic solvent in water or a mixture consisting of water and organic solvent with equivalents of 0.1-5 of a strong Brönsted acid at temperatures of 80-200 DEG C to obtain amino methane phosphonic acid and finally isolating said acid according to the usual methods. This enables high-yield highly pure amino methane phosphonic acid to be produced in a relatively simple manner.
申请公布号 DE19717130(A1) 申请公布日期 1998.10.29
申请号 DE19971017130 申请日期 1997.04.23
申请人 SKW TROSTBERG AG, 83308 TROSTBERG, DE 发明人 NEUMANN, THOMAS, DR., 83308 TROSTBERG, DE;FLEISCHER, FRANK, DR., 83349 PALLING, DE;GRAEFE, JUERGEN, DR., 83308 TROSTBERG, DE;HAMMER, BENEDIKT, DR., 83342 TACHERTING, DE
分类号 C07F9/38;(IPC1-7):C07F9/38 主分类号 C07F9/38
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