发明名称 Method of producing 1,5,5,-trimethyl-6-methylene-1-cyclohexene.
摘要 1. Method of producing 1,5,5,-trimethyl-6-methylene-1-cyclohexene - Characterized in that: β-pyronen is subjected to epoxidation with peracetic acid in the solution of methylene chloride in the presence of anhydrous sodium carbonate at the temperature of 0-25 degrees C, preferably at 0-5 degrees C. The obtained reaction product is treated with BH3 borate, with the molar ration of 3-1 to 2-1, and then with sodium hydroxide. Then, the produced 1,2,6,6-tetramethyl-2-cyclo-hexen-1-yl is dehydrated.
申请公布号 PL174714(B1) 申请公布日期 1998.09.30
申请号 PL19930301072 申请日期 1993.11.15
申请人 UNIWERSYTET MIKOLAJA KOPERNIKA 发明人 ZAIDLEWICZ MAREK;SARNOWSKI RYSZARD;OSUCH PIOTR;KRZEMINSKI MAREK
分类号 C07C13/20 主分类号 C07C13/20
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