摘要 |
Trimethylindium with substantially no oxygen-containing impurities, either as byproduct or associated solvent, is synthesized according to the reaction: MezInX(3-x)+(1-1.2)(3-z)Me3Al+(1-1.2)(6-2z)MF->Me3In+(1-1.2)(3-z)M(Me2AlF2)+(1-1.2)(3-z)MX where the Xs are the same or different and are selected from the group consisting of Cl, Br, and I; M is selected from the group consisting of Na, K, Rb, and Cs; and z is 0, 1 or 2 in a hydrocarbon solvent, such as squalane.
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