发明名称 CHLOROGALLIUM PHTHALOCYANINE CRYSTAL AND PRODUCTION OF DISPERSION LIQUID OF THE CRYSTAL
摘要 PROBLEM TO BE SOLVED: To safely and easily produce the subject crystal having excellent electrophotographic characteristics and useful as an electrophotographic receptor without causing the scattering of impurities by crushing a specific chlorogallium phthalocyanine crystal in a state wet with water, filtering the product and crushing in a state wet with an organic solvent to effect the conversion of the crystal form. SOLUTION: Chlorogallium phthalocyanine having strong diffraction peak at a Bragg angle (2θ) of 27.1±0.2 deg. by CuKαcharacteristic X-ray (e.g. an undried material produced by heating 1,3diiminoisoindoline and gallium trichloride in an organic solvent and washing the obtained condensation reaction product with refined water) is crushed in wet state together with re fined water, filtered and then crushed in wet state using an organic solvent such as n-butyl acetate or dimethyl sulfoxide to convert the original crystal form into the objective crystal form having strong diffraction peaks at 2θ=7.4±0.2 deg., 16.6±0.2' deg., 25.5±0.2 deg. and 28.3±0.2 deg..
申请公布号 JPH1017784(A) 申请公布日期 1998.01.20
申请号 JP19960174458 申请日期 1996.07.04
申请人 FUJI XEROX CO LTD 发明人 TAKIMOTO HITOSHI;HONGO KAZUYA;SUGIYAMA KOICHI
分类号 C07D487/22;C09B67/50;(IPC1-7):C09B67/50 主分类号 C07D487/22
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