发明名称 Butyne-diol preparation from aqueous formaldehyde and acetylene
摘要 A process for the synthesis of butynediol (I) comprises reacting acetylene with an aqueous solution containing formaldehyde, in the presence of a suspended catalyst in a multi-reactor cascade, with solution fed from the first to the second, and so on, and acetylene supplied to each reactor. The amount of catalyst in the solution from each reactor is reduced by 50-99 (preferably 70-97, more preferably 80-95) wt%, before it is fed to the next reactor. A butynediol-rich solution is obtained from the last reactor stage which is separated from the catalyst.
申请公布号 DE19624850(A1) 申请公布日期 1998.01.08
申请号 DE1996124850 申请日期 1996.06.21
申请人 LINDE AG, 65189 WIESBADEN, DE 发明人 DEMBNY, CURD, DIPL.-CHEM. DR., 81369 MUENCHEN, DE;FOERG, WOLFGANG, DIPL.-PHYS., 82057 ICKING, DE;SCHOEDEL, NICOLE, DIPL.-CHEM. DR., 81477 MUENCHEN, DE;LANG, UDO, DIPL.-ING., 81369 MUENCHEN, DE;HAIDEGGER, ERNST, DIPL.-ING. DR., 85635 HOEHENKIRCHEN-SIEGERTSBRUNN, DE
分类号 C07C29/38;(IPC1-7):C07C33/046;C07C29/48;C07C29/74 主分类号 C07C29/38
代理机构 代理人
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